• Issue 10,2022 Table of Contents
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    • >FUNDAMENTAL RESEARCH
    • Effect of egg white powder on frying characteristics of surimi and its mechanism

      2022(10):1-5. DOI: 10.13652/j.spjx.1003.5788.2022.80073

      Abstract (527) HTML (0) PDF 1.63 M (480) Comment (0) Favorites

      Abstract:Objective:The objective of this study is to investigate the effect of egg white powder addition on the fried characteristics of surimi and its influencing mechanism. Methods:The cheap silver carp was used as raw material, and the egg white powder was added to the surimi for compounding. The frying characteristics of surimi were characterized by measuring porosity, hardness and water absorption, and the dynamic rheological properties, foam stability and SDS-PAGE of surimi were measured to explore its influencing mechanism. Results:With the increase of egg white powder content, the porosity and water absorption of fried fish ball increased first and then decreased, and the hardness decreased first and then increased. The effect of 10.0% egg white powder was the best. In addition, SDS-PAGE analysis showed that, new bands with molecular weight of ≥100 kDa were generated in surimi. Accordingly, the porosity of fried fish balls was positively correlated to the gel property and foam stability of surimi. Conclusion:The addition of egg white powder improved the gel property and foam stability of surimi, thereby increasing the stability of pore structure of surimi during frying, improving the porosity and taste of fried fish balls, and improving its edible quality.

    • Effects of hydration temperature, geldosage and potassium chloride dosage on the viscosity of kappa-carrageenan solution

      2022(10):6-10. DOI: 10.13652/j.spjx.1003.5788.2022.90254

      Abstract (817) HTML (0) PDF 1.61 M (564) Comment (0) Favorites

      Abstract:Objective:To achieve accurate application of kappa-carrageenan as a gelling agent in food industries such as processed meats, dairy, desserts and jellies, as well as seamless capsule in pharmaceuticals and crushable beads in tobaccos. Methods: The viscosities of kappa-carrageenan solution prepared at different hydration temperature, different dosages of kappa-carrageenan dosage and potassium chloride were measured by digital viscometer. Results:① The hydration temperature had a great influence on the viscosity of kappa-carrageenan gel solution. With the increasing hydration temperature (fixed hydration time at 1 h), the viscosity of kappa-carrageenan gel solution decreased. Generally the higher the dosage of kappa-carrageenan, the greater the decrease of viscosity. ② The viscosity of kappa-carrageenan solution increased exponentially with increasing dosage. ③ The presence of KCl had little effect on the viscosity at low dosage of kappa-carrageenan. However, the viscosity of kappa-carrageenan solutions at higher dosages increased with the increasing KCl dosage. Conclusion:Hydration temperature and gel dosage had important effects on the viscosity of kappa-carrageenan, while the amount of potassium chloride had relatively little effect on the viscosity.

    • Effects of different concentrations of free SO2 and dissolved oxygen on wine color and anthocyanins content

      2022(10):11-16. DOI: 10.13652/j.spjx.1003.5788.2022.80205

      Abstract (566) HTML (0) PDF 1.58 M (547) Comment (0) Favorites

      Abstract:Objective:This study aimed to explore the effects of different concentrations of dissolved oxygen and free SO2 on the color and related parameters of Cabernet Sauvignon dry red wine during aging, and to provide basic data for enterprises to improve the aging process of Cabernet Sauvignon dry red wine.Methods:Cabernet Sauvignon dry red wine from Xinpuwang Wineyard in Shanshan County, Turpan, Xinjiang was used as the brewing material. The effects of different concentrations of free SO2 and dissolved oxygen on wine color, hue and anthocyanin content were observed during wine aging.Results:The wine was bright red when the concentration of dissolved oxygen and free SO2 was low. When the content of oxygen was 2 mg/(L·30 d), the moderate polymerization of anthocyanin and tannin in wine was promoted, and the quality of the wine was improved. When the concentration of free SO2 was 15 ~ 30 mg/L, it had little effect on the hue value of grape wine, but it had an obvious effect on the color. When the concentration of free SO2 was more than 30 mg/L, the color of grape wine gradually became orange.Conclusion:The suitable concentration of free SO2 for Cabernet Sauvignon dry red wine aging was 25 mg/L, and the oxygen content was 2 mg/(L·30 d).

    • Tomato weight prediction based on image processing

      2022(10):17-23. DOI: 10.13652/j.spjx.1003.5788.2022.90159

      Abstract (315) HTML (0) PDF 2.11 M (554) Comment (0) Favorites

      Abstract:Objective:A tomato weight detection method based on image processing was established to realize non-contact tomato weight detection. Methods:The binary image of tomato was obtained through image processing. The geometric features of tomato were extracted by pixel statistics and minimum circumscribed rectangle method, and correlation analysis was made between the characteristics and the real value of tomato weight, then the regression model of tomato weight detection with geometric features as parameters was established. Results:Compared with the real size of tomato, the measurement error of transverse and longitudinal diameter of Tomato by minimum external rectangle method was less than 3%. In addition to fruit shape index, other geometric characteristics were linearly correlated with tomato fruit weight, and the correlation between positive characteristics and fruit weight was more significant. Three types of 20 models were established for prediction and evaluation. The multiple regression model with the parameters of tomato front projection area and perimeter, projection area of a side image and tomato transverse diameter had the highest accuracy, the regression coefficient was 0.962, the average relative error of detection value was 0.673%, and the average absolute error was 1.425 g. Conclusion:The model is suitable for the weight detection of tomatoes and other fruits or articles with similar axisymmetric shape characteristics.

    • Primary structure characterization and antioxidant activity of polysaccharide from Zizyphus jujuba cv. Banzao

      2022(10):24-28. DOI: 10.13652/j.spjx.1003.5788.2022.90206

      Abstract (227) HTML (0) PDF 1.64 M (475) Comment (0) Favorites

      Abstract:Objective:This study aimed to analyze the physicochemical properties, primary structure and antioxidant activity of polysaccharide from Zizyphus jujuba cv. Banzao.Methods:The polysaccharides were prepared by water extraction and alcohol precipitation, deproteinization with trichloroacetic acid and decolorization with hydrogen peroxide. The physicochemical properties of polysaccharides were studied, and the possible structures were predicted by Ultraviolet-visible (UV-Vis) and infrared (IR) spectroscopy. Finally, the free radical scavenging ability was determined.Results:The polysaccharide from Z. jujuba cv. Banzao contained the content of total sugar and uronic acid with 52.30% and 46.22%, respectively, and showed 64.70% of esterification degree, which was an acidic pectin polysaccharide; UV-VIS and IR spectroscopy showed that the polysaccharide from Z. jujuba cv. Banzao had typical polysaccharide absorption peak, and contained no protein or nucleic acid. It was a pyranose with α-glycosidic bond, mainly composed of galacturonic acid, galactose, arabinose, glucose. The polysaccharides from Z. jujuba cv. Banzao displayed certain antioxidant activity and the free radical clearance of the polysaccharide at 1 mg/mL for DPPH radical, ·OH and ABTS+· were 23.64%, 21.01% and 13.84%, respectively.Conclusion:The polysaccharide from Z. jujuba cv. Banzao was an acidic pectin sugar mainly composed of galacturonic acid. Besides, it had α-glycosidic bond and showed strong antioxidant capacity, which can be used as a potential antioxidant.

    • Construction of evaluation model of volatile flavor intensity of cyclic stewed beef based on principal component analysis

      2022(10):29-36. DOI: 10.13652/j.spjx.1003.5788.2022.90111

      Abstract (309) HTML (0) PDF 1.51 M (466) Comment (0) Favorites

      Abstract:Objective:In order to evaluate the difference of characteristic flavor intensity between different times of cyclic stewed beef.Methods:The volatile flavor compounds in circulating stewed beef were determined by solid phase microextraction-gas chromatography-mass spectrometry (SPME-GC-MS), and the key flavors with important contribution were screened out according to the relative odor activity value. The flavor substances contributed by circulating stewed beef were analyzed by principal component analysis, the flavor intensity evaluation model of cyclic stewed beef was established, and the comprehensive evaluation of cyclic stewed beef was carried out combined with sensory evaluation.Results:The seven key flavourings were n-hexanal, undecanal, nonanal, n-hexanol, 3-methylpentane, cineole and anethole. The results showed that the contribution rates of the first to third principal components obtained by principal component analysis were 52.40%, 25.64% and 12.95% respectively, and the cumulative contribution rate was 90.98%, which could represent the main information of volatile flavor substances in cyclic stewed beef. The correlation coefficient between the characteristic flavor intensity of the model and the sensory score was 0.90(P<0.05).Conclusion:The model can be applied to the flavor evaluation of cyclic stewed beef.

    • Effects of the dark blue pigment from Vaccinium bracteatum Thunb leaves on the physicochemical properties of rice protein

      2022(10):37-42. DOI: 10.13652/j.spjx.1003.5788.2022.60081

      Abstract (629) HTML (0) PDF 1.54 M (474) Comment (0) Favorites

      Abstract:Objective:This study was to explore the improvement of structural and emulsifying properties of rice protein by interacted with the dark blue pigment of Vaccinium bracteatum Thunb leaves. Methods:The dark blue pigment was prepared from VBTL, and the changes of structural and emulsifying properties of rice protein before and after dyeing were analyzed. Results:The formation of binary complexes between the dark blue pigment and the rice protein decreased the color values of L* and b*, and the hue of the pigment-protein complex changed to dark blue color with the increase of the pigment concentration. The water solubility of the pigment-protein complex increased, and the oil-holding capacity decreased significantly. The analysis circular dichroism spectroscopy showed the changes in the secondary structure of pigment-protein complex with a decreasing in the relative content of α-helices and β-folds and an increasing in the relative content of β-turns and random coil. At the concentration of pigment below 1.5%, foam stability increased, while foaming capacity, emulsifying capacity and emulsion stability decreased. When the concentration of pigment was higher than 1.5%, foam stability decreased, while foaming capacity, emulsifying capacity and emulsion stability increased. Conclusion:The dark blue pigment can improve the emulsifying properties of rice protein by changing its secondary structure.

    • Effects of glycerol application ratio on the distribution of moisture, nicotine and glycerol in heated cigarettes

      2022(10):43-49. DOI: 10.13652/j.spjx.1003.5788.2022.90120

      Abstract (796) HTML (0) PDF 1.86 M (686) Comment (0) Favorites

      Abstract:Objective:In order to optimize the process parameters of tobacco sheet of heated cigarette. Methods:12 gradient grades of tobacco sheets with glycerol addition ratio of 5%~30% were prepared under laboratory conditions. The mass of moisture, nicotine and glycerol in heated cigarette smoke, filter condensation section and tobacco core section were detected by GC-TCD method. And the mass distribution characteristics of main components, release rate, filtration rate and transfer rate were analyzed. Results:When 5%~30% glycerol was applied to the heated cigarette tobacco sheets, the water release rate was 88.6%~92.3%, which was mainly distributed in the smoke and filter condensation section; The nicotine release rate was 25.5%~34.2%, which was mainly distributed in the filter condensing section and tobacco core section; The glycerol release rate was 13.9%~21.3%, which was mainly distributed in the tobacco core section. Conclusion:When 10%~18% glycerol was added to tobacco sheets, nicotine and glycerol in heated cigarettes had higher transfer rate and lower filtration rate.

    • >SAFETY & INSPECTION
    • Determination of iodine in milk powder by combing microwave digestion with inductively coupled plasma mass spectrometry

      2022(10):50-54. DOI: 10.13652/j.spjx.1003.5788.2022.90188

      Abstract (655) HTML (0) PDF 1.39 M (401) Comment (0) Favorites

      Abstract:Objective:This study aimed to establish an efficient and accurate method for the determination of total iodine in milk powder by microwave digestion combining with inductively coupled plasma mass spectrometry (ICP-MS). Methods:Firstly, 0.2 mL of precipitant and 5 mL of ultrapure water were added for mixing and standing, and then 5 mL of nitric acid was added for microwave digestion. After cooling, the volume was fixed to 35 mL with ultrapure water, and then 10 mL of ammonia, 1 mL of stabilizer and 50 μL of TritonX-100 were added in sequence, avoiding the iodine loss. Results:The detection limit was 0.044 mg/kg,while iodine presented favorable linearity in the range of 0~20 μg/L with correlation coefficient (r) of 0.999 9. The precision of the method (RSD %) was less than 5%, and the spiked recoveries of real samples is 90.2% ~ 107.7%. The measured values of various standard substances are consistent with the labeled values. The iodine content of the same milk powder was similar to that of GB 5009.267—2020. Conclusion:The method showed the advantages of high efficiency, good recovery and accurate for the determination of iodine contents in milk powder, ensures personnel safety and reduces instrument maintenance cost.

    • Uncertainty evaluation for determination of isocarbophos residues in tea by QuEChERS-gas chromatography-tandem mass spectrometry

      2022(10):55-60. DOI: 10.13652/j.spjx.1003.5788.2022.90186

      Abstract (655) HTML (0) PDF 1.45 M (436) Comment (0) Favorites

      Abstract:Objective:The uncertainty of determination of Isocarbophos residues in tea by using QuEChERS-gas chromatography-tandem mass spectrometry techniqne was evaluated. Methods:Isocarbophos residues in tea was determined by using "GB 23200.113—2018 National food safety Standard-Determination of 208 pesticides and metabolites residues in plant origin-Gas chromatography-tandem mass spectrometry method", and factors in the determination of isocarbophos were analyzed by establishing a mathematical model, including sample weighing, volume, calibration of standard solutions, repeatability and recovery rate, etc.. Results:When the residual amount of isocarbophos in tea was 0.050 mg/kg, the expanded uncertainty was 0.007 mg/kg, and the determination result was expressed as:ω=(0.050±0.007) mg/kg,k=2. Conclusion:The main sources of uncertainty in this method werecalibration of standard solutions and the recovery rate.

    • Visualization of lamb adulteration based on hyperspectral imaging for non-destructive quantitative detection

      2022(10):61-68. DOI: 10.13652/j.spjx.1003.5788.2022.90174

      Abstract (566) HTML (0) PDF 2.48 M (427) Comment (0) Favorites

      Abstract:Objective: This study aimed to establisha rapid and accurate prediction method of lamb adulteration by using visible/near-infrared (400~1 000 nm) and short-wave near-infrared (900~1 700 nm) hyperspectral imaging techniques.Methods: The data acquisition of lamb adulterated with different proportions of duck meat using visible/near-infrared (400~1 000 nm) and short-wave near-infrared (900~1 700 nm) hyperspectral imagers was performed to compare the effect of partial least squares (PLS) modeling with different spectral preprocessing methods in the two band ranges. Then the normalized preprocessing method was selected in the visible-NIR band, and the standard normal variate transformation (SNV) preprocessing method was selected in the short-wave infrared band. After the optimal preprocessing of the spectral data on to the two bands separately, the feature wavelengths were selected using the successive projections algorithm (SPA), the competitive adaptive reweighted sampling (CARS), the Interval random frog (iRF) and the Synergy intervals PLS (SiPLS).Results: The best lamb adulteration prediction using SNV-SPA-PLS model in the short-wave near-infrared (900~1 700 nm) bands, was achieved, and with the prediction set model evaluation coefficients of R2p=0.968 4, RMSEP=0.058 2, RPD=5.625 4, relaiable image inversion results were obtained.Conclusion: The rapid and nondestructive quantitative detection of lamb adulteration can be achieved by using hyperspectral imaging techniques in different wavebands.

    • Construction and application of a comprehensive evaluation index system for food safety

      2022(10):69-75. DOI: 10.13652/j.spjx.1003.5788.2022.80397

      Abstract (491) HTML (0) PDF 1.92 M (572) Comment (0) Favorites

      Abstract:Objective:This study aimed to build a unified and standardized comprehensive food safety evaluation index system. Methods: The research status of the comprehensive evaluation index domestic and abroad system of food safety were summarized from two levels of theoretical research and practical exploration. Results: Based on the analytic hierarchy process and Delphi method, a set of comprehensive evaluation index system of food safety with 6 criteria, 24 first-level indicators and 41 secondary indicators was constructed; this set of indicators combined with relevant statistical data was used to carry out an empirical analysis of the food safety situation in various administrative districts of Tianjin. Conclusion: Practice shows that this set of indicators can effectively evaluate and compare the food safety status of various districts, and has the advantages of comprehensiveness, practicality and comparability.

    • Analysis of pesticide residues and heavy metal pollution in leek

      2022(10):76-81. DOI: 10.13652/j.spjx.1003.5788.2022.60076

      Abstract (656) HTML (0) PDF 1.42 M (469) Comment (0) Favorites

      Abstract:Objective:This study aimed to help with the scientific management of leek food safety in Hunan Province. Methods: 24 kinds of pesticides and 5 kinds of heavy metals in 690 leek samples from Hunan Province were detected. Results:① Pesticide residues were detected in 23.19% of the 690 samples, and the top three pesticides were determined to be carbendazim, procymidone and cypermethrin. The exceeding rate of pesticide residues was 5.80%, and the highest exceeding rate was 2.61% of procymidone. ② The detection rate of heavy metal elements was 77.68%, and the exceeding rate was 3.62%. The highest detection rate and exceeding rate of heavy metal elements was Cd. Conclusion: High pesticide residues in leek were confirmed, and the detection rate of heavy metal elements in leeks is much higher than that of pesticide residues. Among them, pesticide procymidone and heavy metal Cd are the main over-standard items of leeks. It is suggested to strengthen the continuous monitoring of pesticide residues and heavy metal pollution in leeks.

    • Determination of three methylimidazole compounds in food flavors by solid phase extraction coupled with ultra-performance liquid chromatography-mass spectrometry

      2022(10):82-86. DOI: 10.13652/j.spjx.1003.5788.2022.90198

      Abstract (617) HTML (0) PDF 1.58 M (363) Comment (0) Favorites

      Abstract:Objective: This study aimed to establish a method for quick determination of 3 kinds ofmethylimidazole compounds in food flavor. Methods:The food flavor was extracted with 5% trichloroacetic acid solution and purified with PCX mixed cationic solid phase extraction column. Finally, the qualitative and quantitative analysis was carried out by ultra- performance liquid chromatography-mass spectrometry (UPLC-MS/MS) and internal standard method. Results: The linear relationship between the three methyl imidazole compounds was good in the range of 5.0~400.0 ng/mL, with correlation coefficient R2≥0.997. The limits of detection were 0.030~0.450 μg/kg and the limits of quantification (LOQ) were 0.10~1.50 μg/kg. The recoveries of three methylimidazole ranged from 82.8% to 111.7%, and the relative standard deviations (RSDS) ranged from 1.3% to 9.3%. Conclusion:The method is simple, efficient and accurate, and can be used for the quantitative determination of 1-methylimidazole, 2-methylimidazole, 4-methylimidazole in food flavor.

    • Research on quantitative fish segmentation method based on line laser scanning

      2022(10):87-92. DOI: 10.13652/j.spjx.1003.5788.2022.90197

      Abstract (303) HTML (0) PDF 2.20 M (518) Comment (0) Favorites

      Abstract:Objective:To realize the mechanization of quantitative cutting of fish before processing fish products. Methods:Obtained the fish contour data by linear laser scanning, the distribution of fish body weight with body length was obtained. The quantitative cutting models of fish body with fixed weight and equal weight were constructed, and the validity and accuracy of the method were verified by experiments. Results:The results showed that the predicted curve of fish body weight distribution was close to the real distribution curve, the accuracy of 10 fish was above 91%. The mean absolute errors were 0.16, 0.38 and 1.15 g, respectively. For a given segment weight of 10, 15 and 20 g, the mean absolute errors of 10, 15 and 20 segments were 2.44, 1.35 and 0.67 g, respectively. Conclusion:The research results provide a feasible idea for quantitative segmentation processing of fish, and provide a theoretical reference for the development of intelligent fish processing machinery.

    • Design of on-line nondestructive rapid detection system for tilapia descaling rate based on machine vision

      2022(10):93-98. DOI: 10.13652/j.spjx.1003.5788.2022.90199

      Abstract (89) HTML (0) PDF 3.27 M (443) Comment (0) Favorites

      Abstract:Objective:Improve the quality and efficiency of tilapia processing and increase the added value of products.Methods:For the fluorescence response difference of fish scales and fish skin under ultraviolet excitation, a rapid detection system for tilapia descaling rate based on machine vision technology was constructed. After image pre-processing, background segmentation, ROI region selection, and rapid identification of discaled areas, the scaled and descaled area images were obtained. Then the scaling rate was calculated and the detection accuracy of the system was tested. Results:The accuracy of the system scaling rate detection ranged from 90.18% to 94.14%.Conclusion:The automatic transmission of the tilapia sample, the automatic triggering and acquisition of the detection image, the rapid image processing can be realized by the system, which can effectively improve the detection efficiency of tilapia descaling rate and meet the requirements of the production line.

    • The design of 3D icing sugar printer based on room temperature extrusion

      2022(10):99-103. DOI: 10.13652/j.spjx.1003.5788.2022.80003

      Abstract (698) HTML (0) PDF 2.10 M (425) Comment (0) Favorites

      Abstract:Objective:The paper aims to design a 3D icing sugar printer that meets the requirements of safety, hygiene, convenient operation, and stable structural performance. Methods:The 3D icing sugar printer includes the mechanical mechanism and control system. The mechanical structure adopts a gantry structure and reforms the food can. The control system adopts "Industrial PC + Motion control card" mode. Results:Fast food can replacement (< 30 s); fast printing speed (≥5 000 mm/min), adjustable speed; printing accuracy (<1 mm); good strength, expansion rate and surface roughness of the printed objects. The image recognition and processing system with the self-light source can identify the shape, number and integrity of the printing objects. Conclusion:The reformed food can improves the hygiene, production efficiency of semi-fluid food printing and is replaced quickly. The 3D icing sugar printer has stable structural performance and convenient operation, and can print icing sugar products that meet different design requirements.

    • Development of single-piece ham package defect recognition and sorting system based on parallel robot

      2022(10):104-109. DOI: 10.13652/j.spjx.1003.5788.2022.60080

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      Abstract:

      Objective: Improve the sorting effect of single-piece ham package. Methods:Combined with automatic control, machine vision and other technologies, a sorting system capable of identifying single-chip ham defects was designed based on a Delta parallel robot. The kinematics and dynamics model of 2-DOF Delta parallel robot was established, and then the Delta parallel robot was optimized. The composition of control system and the algorithm of image processing were designed. Results: The system can successfully identify impurities and creases, with the recognition rate of up to 95%. It can also accurately and efficiently sort single-piece ham package, with the sorting success rate of more than 98%, and the sorting efficiency of more than 160 packets per minute. Conclusion: The sorting system can realize continuous operation of identification, grasping, handling, sorting and eliminating.

    • Research status and prospect of key technologies for automatic production of fresh and wet rice flour

      2022(10):110-117. DOI: 10.13652/j.spjx.1003.5788.2022.90209

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      Abstract:Firstly, this paper expounds the research status at home and abroad of three key technologies in the production process of fresh and wet rice flour: efficient powder dispersion, accurate weighing and automatic packaging, and focuses on the key technical problems existing in the research and development of technology and mechanical equipment; Secondly, on the basis of summarizing the development level of existing technology and equipment, this paper further analyzes the main reasons for these problems. Finally, the development direction of three key technologies in the automatic production of fresh and wet rice flour is prospected from the aspects of production technology, mechanical design and system algorithm optimization.

    • >包装与设计
    • Study on migration mechanism of sweeteners in tipping paper

      2022(10):118-122. DOI: 10.13652/j.spjx.1003.5788.2022.60083

      Abstract (251) HTML (0) PDF 1.66 M (400) Comment (0) Favorites

      Abstract:Objective:This study aimed to solve the problem of cigarette flavoring technology that the surface taste of splicing paper weakens over time. Methods:A rapid method for the simultaneous determination of two kinds of sweeteners was established based on ultra-high-performance liquid chromatography (UHPLC). The change of the content of the sweetener on the surface of the tipping paper was analyzed, and the induced migration experiment was used to analyze the migration of sweeteners. The surface porosity, air permeability and surface water absorption of aluminized splice paper were analyzed by scanning electron microscope, air permeability tester and surface water absorption tester. Results:A method for rapid determination of two kinds of sweeteners simultaneously was established by UHPLC. The results of induced migration experiment showed that the sweeteners in the tipping paper migrated from the surface to the inside of the paper gradually. The results of scanning electron microscope, air permeability tester and surface water absorption tester showed that pores distributed on the surface of the aluminized tipping paper, and the high air permeability thereby led to the surface water absorption capacity. Therefore, the sweetener migrated in the aluminized tipping paper. After 42 days of induced migration, the migration rates of acesulfame and saccharin sodium in the paper were 48.47% and 49.65%, respectively. Conclusion: The pores and cracks spreading on the surface of the aluminized tipping paper made it have high permeability and strong water absorption, and the concentration differences between the two sides of the paper resulted in a conducive migration of the sweeteners.

    • Application of story elements in children's food packaging design based on cognitive psychology

      2022(10):123-126. DOI: 10.13652/j.spjx.1003.5788.2022.60065

      Abstract (471) HTML (0) PDF 2.29 M (393) Comment (0) Favorites

      Abstract:This paper analyzes the problems existing in the current packaging design of children's food in China, and studies the emotional value, intellectual value, information transmission value and brand value of story elements in the packaging design of children's food. Explores the specific application of story elements in the packaging design of children's food from three aspects, namely, the theme of the incident, the scenario of the story, and the plot design, with the help of several award-winning international packaging works in recent years.

    • >STORAGE TRANSPORTATION & RESEARCH
    • Effects of 1-MCP combined with low temperature storage on postharvest physiology and quality of Zaoshengxinshui pear

      2022(10):127-133. DOI: 10.13652/j.spjx.1003.5788.2022.90183

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      Abstract:Objective:This study focused on fresh-keeping technology with quality control as the main factor.Methods:The respiratory climacteric Zaoshengxinshui pear was used as material, after being fumigated with 3.24 μL/L of 1-MCP, then was stored at (10±1) ℃. The fruits stored at (10±1) ℃ and (1±1) ℃ without any treatment were used as control 1 (CK1) and control 2 (CK2). The respiration intensity, ethylene release rate, firmness, soluble solid content, peel chromatism, core browning index, weight loss rate and decay rate of fruits during postharvest storage were measured and investigated, and the correlation was analyzed.Results:Compared with CK1, (10±1) ℃ combined with 1-MCP treatment could inhibit the ethylene release rate and respiratory intensity of fruit, delay its peak, but the inhibition effect on respiration intensity and ethylene release rate were still significantly lower than that of CK2. It can maintain high soluble solid content, reduce fruit water loss, delay fruit decay and browning, maintain the green peel (absolute value of a* was high,h° was high). During the whole storage time, the peel hardness, pulp hardness, fruit brittleness and pulp compactness of fruits treated with (10±1) ℃ combined with 1-MCP were significantly higher than those of CK1. However, the retention effect of CK2 on fruit parenchyma was still higher than of (10±1) ℃ combined with 1-MCP; except respiration intensity, ethylene release rate and brown heart index, there were different degrees of correlation among other indexes.Conclusion:The safe storage period of (10±1) ℃ combined with 3.24 μL/L 1-MCP fumigation can reach 103 days, and the soluble solids are stable at about 12%. Therefore, it can better maintain the. inherent flavor and color of the fruit, which can be used as one of the fresh-keeping technologies instead of single low-temperature storage.

    • Effects of slightly acidic electrolytic water on blueberry sterilization process and storage quality

      2022(10):134-138. DOI: 10.13652/j.spjx.1003.5788.2022.90208

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      Abstract:Objective:To improve the preservation quality of blueberry.Methods:Based on the influencing factors of the effective chlorine concentration, treatment temperature and soaking time of the SAEW, and the response value of the microbial sterilization rate on the surface of blueberries, the orthogonal test was used to optimize the process conditions. At the same time, the optimally treated blueberries and sterile water-treated blueberries (control group) were stored at (25±1) ℃, and the bad fruit rate, hardness, respiration strength, soluble solids content, titratable acid content, anthocyanin content, and malondialdehyde (MDA) content of blueberries were measured every 7 days.Results:The optimal sterilization conditions were an effective chlorine concentration of 120 mg/L, a treatment temperature of 20 ℃ and a soaking time of 20 min, and the sterilization rate under this condition was 92.6%.Conclusion:The SAEW treatment has a better preservation effect on the blueberry fruit.

    • Effects of drying methods on the quality and microstructure of Armillaria luteo-virens

      2022(10):139-145. DOI: 10.13652/j.spjx.1003.5788.2022.80248

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      Abstract:Objective:This study aimed to determine the most suitable drying method for Armillaria luteo-virens.Methods:The effects of solar drying, hot air drying, vacuum-freeze drying, vacuum drying and microwave-hot-air combined drying on the nutrition, functional components, color, rehydration ratio, shrinkage ratio, rehydration structure and microstructure of A. luteo-virens were compared.Results:The content of crude protein, crude polysaccharide and total flavonoids in vacuum-freeze drying group was the highest, and the content of total phenol was second highest and lower than the vacuum drying group. Its color difference was the smallest, with high rehydration ratio, and the shrinkage degree was small, with good internal tissue integrity. Moreover, its rehydration structure was characterized by low hardness, elasticity and chewability. Compared with hot-air drying, microwave-hot-air combined drying significantly increased the content of crude protein and crude polysaccharide of A. luteo-virens, shortened the drying time by 11%, and significantly improved the b* value; after rehydration, its hardness, elasticity, cohesion and chewability were the largest. However, the vacuum drying group was not conducive to the retention of total flavonoids, and had the worst performance in shrinkage and rehydration; the crude fiber content was the highest and the total phenol content was the lowest in the solar drying group.Conclusion:Different drying methods have significant effects on the quality of A. luteo-virens, and the overall quality of vacuum-freeze drying A. luteo-virens is optimal.

    • Effect of compound preservatives on Orah fruits storage quality

      2022(10):146-150. DOI: 10.13652/j.spjx.1003.5788.2022.90225

      Abstract (993) HTML (0) PDF 1.64 M (1727) Comment (0) Favorites

      Abstract:Objective:This study aimed to investigate the effects of different concentrations of preservatives on storage quality of orah fruits, so as to reduce the use of preservatives during its planting.Methods:The weight loss rate, vitamin C content, soluble solid content and titratable acid content of fruits were determined under different storage conditions, by using different concentrations of preservative.Results:At 4 ℃ and room temperature, the weight loss rate of fruits treated with preservatives was lower than that of the control group, and preservative treatment had different fresh-keeping effects on orah fruits. At 4 ℃, significant differences in vitamin C content among different treatments at 5, 28 and 42 days of storage were found, but no significant differences in other storage time. No significant difference in soluble solids and titratable acid contents among different treatments appeared. Among the treatment groups (treatment 1, treatment 2 and treatment 3), the weight loss rate, vitamin C content, soluble solid content and titratable acid content of orah fruit in treatment 2 were better than those in treatment 1 and 3. At room temperature, vitamin C content was significantly different among different treatments on the third day of storage. After 14 days of storage, the soluble solid content of treatment groups 1 and 2 was significantly different. On the 14th day of storage time, titratable acid content in treatment group 2 was significantly higher than that in treatment group 3. The contents of vitamin C, soluble solids and titratable acid in treatment group 2 were higher than those in other treatment groups, during most storage time.Conclusion:At 4 ℃, each preservative treatment has different degrees of preservation effect on orah fruits. 450 g/L midazamine +500 g/kg statin +100 g/kg 2,4-D+400 g/kg bellkute has better preservation effect on orah fruit.

    • >EXTRACTION & ACTIVITY
    • Optimization of calcium removal in the carapace of Chinese soft-shelled turtle and structural characteristics of its collagen

      2022(10):151-157. DOI: 10.13652/j.spjx.1003.5788.2022.90219

      Abstract (642) HTML (0) PDF 1.82 M (456) Comment (0) Favorites

      Abstract:Objective:To improve the extraction rate and product purity of Chinese soft-shelled turtle (pelodiscussinensis)dorsal collagen. Methods:The decalcification rate and collagen recovery rate were used as evaluation indicators to investigate the effects of hydrochloric acid concentration, decalcification time, decalcification temperature and solid-liquid ratio on the decalcification of the carapace of Chinese soft-shelled turtle. The removal process of calcium salts was optimized, and the structural changes of decalcified and non-decalcified turtle carapace collagen were analyzed by SDS-PAGE, ultraviolet absorption spectroscopy, infrared absorption spectroscopy, amino acid analysis and other techniques under the same extraction conditions. Results:The optimal decalcification process conditions were hydrochloric acid concentration of 0.8 mol/L, decalcification time of 2 h, decalcification temperature of 28 ℃, and solid-liquid ratio of 1∶25 (g/mL). Under these conditions, the decalcification rate and collagen recovery rate were (67.35±0.92)% and (90.77±1.08)%, respectively. The collagen content and extraction rate per unit mass of soft-shelled turtle carapace were significantly increased (P<0.05) after decalcification with hydrochloric acid, but the structural characteristics of collagen did not change significantly. Conclusion:Hydrochloric acid has a good decalcification effect on the decalcification of turtle carapace, and has no effect on the structural properties of its collagen.

    • Optimization of recrystallization process of flavonoids from Guanxi pomelo

      2022(10):158-163. DOI: 10.13652/j.spjx.1003.5788.2022.80115

      Abstract (377) HTML (0) PDF 2.19 M (333) Comment (0) Favorites

      Abstract:Objective:This study aimed to improve the recrystallization yield and purity of flavonoid.Methods:Taking the crude flavonoids from pomelo peel extracted by ultrasonic-assisted ethanol extraction as raw materials, the process parameters of ethanol recrystallization and purification of flavonoids were optimized by response surface methodology.Results:The main factors affecting the recrystallization yield of flavonoids were ethanol concentration, crystallization time, pH value, and the interaction between ethanol concentration and pH value, among which, the ethanol concentration affacted most significantly.Conclusion: The optimal recrystallization conditions of flavonoids were as follows: ethanol volume fraction of 24%, liquid-solid ratio of 10∶1 (mL/g), pH 3.75, crystallization temperature of 4 ℃, and crystallization time of 24 h. The crystallization yield of flavonoids was 8.76%, and the main crystallization product was naringin with a purity of 83.38%.

    • Optimization of alcohol extraction process and in vitro lipid-lowering effects of Puerariae lobata

      2022(10):164-170. DOI: 10.13652/j.spjx.1003.5788.2022.80106

      Abstract (121) HTML (0) PDF 2.37 M (255) Comment (0) Favorites

      Abstract:Objective:This study focused on exploring thein vitrolipid-lowering efficacy of Puerarin lobata extract.Methods: The adsorption ratios of oil, cholesterol, sodium glycocholate and sodium taurocholate were evaluated by a multi index comprehensive scoring method to optimize the P. lobata alcohol extraction process using Box-Behnken response surface methodology with extraction time, extraction times and ethanol concentration as influencing factors.In vitro lipid-lowering activity was further validated by comparing the levels of TG and TC accumulation and the extent of intracellular lipid droplet accumulation in a model of human hepatoma (HepG2) fatty liver cells induced by palmitic acid (PA).Results: The optimal alcohol extraction process of P. lobata was 70% by volume of ethanol, 1 h of extraction time and 3 times of extraction time;P. lobata extract could obviously reduce the contents of TG and TC in cells and effectively reduce the intracellular lipid droplet aggregation.Conclusion: The optimized P. lobata extraction process was stable and reliable, manipulable, and showed good lipid-lowering activity in vitro.

    • Optimization on extraction technology of bacteriostatic extract from Indocalamus leaves and its bacteriostatic test

      2022(10):171-177. DOI: 10.13652/j.spjx.1003.5788.2022.80164

      Abstract (649) HTML (0) PDF 1.54 M (295) Comment (0) Favorites

      Abstract:Objective:To study and optimize the extraction technology of bacteriostatic extract from Indocalamus leaves. Methods:The extracts were drawn from Indocalamus leaves by ultrasound-assisted, refluxing and immersing method with extraction solvents: water, ethyl acetate, pH 4 of hydrochloric acid solution, pH 4 of acetic acid solution, pH 10 of ammonia solution and different volume ratio ethyl alcohol. The tests were carried out to analyze the antimicrobial effects with indicator bacteria Bacillus subtilis, Pseudomonas aeruginosa, Shigella Dysenteriae and Salmonella typhi and the total bacteriostatic circle was as inspection indicator, to find out the best extraction solvent and the best extraction method. Using water as extraction solvent, ultrasonic extraction method as method, an orthogonal test L9(33) was carried out by adjusting three impact factors. The impact factors were liquid-solid ratio, sonication period and sonication frequency. The orthogonal test found the optimal extraction process parameters and obtained the best extract. At the same time, the antimicrobial effect of the extract obtained under the optimized conditions was investigated according to the standard series of reference substances. Results:The results showed that water was the best solvent, and ultrasound-assisted method was the best method. The best extraction process parameters were as follows: the ratio of liquid to solid was 16∶1(mL/g), ultrasonic frequency was 4 times, ultrasonic period was 55 minutes. The inhibitory effect of the best extract on Bacillus Subtilis and Salmonella Typhi was equivalent to the effect of 0.01 and 0.03 mg/mL gentamicin, respectively. The bacteriostatic effects on Pseudomonas Aeruginosa and Shigella Dysenteriae were greater than that of 0.05 mg/mL gentamicin. Conclusion:The water ultrasonic method is an effective method for extracting antibacterial substances from Indocalamus leaves, and the inhibitive effect of the extract on Bacillus Subtilis,Pseudo monas Aeruginosa,Shigella Dysenteriae and Salmonella Typhi is remarkable.

    • Study on extraction and pyrolysis analysis of newphytodiene in tobacco leaves

      2022(10):178-186. DOI: 10.13652/j.spjx.1003.5788.2022.90156

      Abstract (739) HTML (0) PDF 1.57 M (389) Comment (0) Favorites

      Abstract:Objective:In order to clarify the heat release behavior of neophytadiene under different conditions.Methods:Use Soxhlet extraction method, chromatography column method to extract and purify neophytadiene in tobacco powder, combined with IR, 1H NMR and MS spectrum technology, the structure was confirmed, and Py-GC/MS was used to analyze and study the pyrolysis products of neophytadiene under different conditions.Results:The performance of neophytadiene at different temperatures under anaerobic and aerobic conditions had good cracking thermal stability, and it can still maintain its original state at high temperature. The types of new phytadiene cracking products increased with the increasing of temperature. Under anaerobic conditions, the anaerobic cracking products of cracking products mainly include alkanes and alkenes. In addition to alkanes and alkenes, the main products of cracking under aerobic conditions also produce a large amount of alcohols, aldehydes, ketones, esters, benzene series, and other compounds. Under aerobic conditions, the neo phytadienes were cracked Alcohols, aldehydes, ketones, esters, furans and other compounds containing oxygen atoms, these components have a positive effect on improving the smoking quality of cigarettes. The formation of cracked products mainly comes from primary and secondary reactions The primary reaction of neophytadiene is mainly the scission of α and β bonds of conjugated double bonds, and the secondary reaction is relatively complicated.Conclusion:Neophytadiene has a positive effect on improving the smoking quality of cigarettes.

    • Protective effects of the pea ACE inhibitory peptide on induced damage of EA.hy.926 cells

      2022(10):187-193. DOI: 10.13652/j.spjx.1003.5788.2022.90213

      Abstract (204) HTML (0) PDF 1.50 M (320) Comment (0) Favorites

      Abstract:Objective:This study aimed to realize the high-value utilization of pea protein.Methods:Using pea protein as raw material, ACE inhibitory peptide derived from pea protein was prepared by double-enzyme coordinated enzymatic hydrolysis method, and the ACE inhibition rate, hydrolysis degree and soluble protein content of the hydrolysate were used as indicators to determine the best enzymatic process for the pea ACE inhibitory peptide. Then the ACE inhibitory peptides produced under the optimal enzymatic digestion process were graded by ultrafiltration to explore the effect of molecular weight on the ACE inhibitory activity. Finally, the protective effect of the pea peptide with high ACE inhibitory activity against the injured EA.hy.926 cells was verified by measuring ET-1, MDA content, SOD and NO content levels.Results:The optimal preparation conditions of pea ACE inhibitory peptide by double-enzyme method were as follows: substrate concentration of 100 mg/mL, 3.0% alcalase enzymolysis for 2.0 h at pH 9.5 and 50 ℃, and then adding 3.0% compound protease for 2.0 h at pH 7.0 and 50 ℃. Under these conditions, the IC50 value of ACE inhibition rate of pea protein hydrolysate was 1.141 mg/mL. Peptide components less than 2.5 kDa had the strongest ACE inhibitory activity and could significantly reduce ET-1, MDA content and increase SOD and NO content levels of Ang-induced injured cells.Conclusion:The pea ACE inhibitory peptide was protective against Ang-induced damage to EA.hy.926 cells.

    • >DEVELOPMENT & APPLICATION
    • Optimization of puffing process of blueberry residue composite indica rice and its antioxidant activity

      2022(10):194-200. DOI: 10.13652/j.spjx.1003.5788.2022.90217

      Abstract (332) HTML (0) PDF 1.62 M (311) Comment (0) Favorites

      Abstract:Objective: This study aimed to research and develop puffed blueberry dregs indica rice and fruit snack food. Methods: Using indica rice flour and blueberry residue powder as raw materials, three experimental factors including moisture content, extrusion temperature and screw speed were selected, and the expansion degree, anthocyanin content and sensory score were taken as comprehensive indexes. The expansion process was optimized by single factor and orthogonal test, and the antioxidant activity of the expanded products was studied. Results: The optimum process parameters were as follows: the moisture content of the material was 16%, the temperature of the four extrusion zones were 50—80—110—130 ℃ and the screw speed was 160 r/min.The indica rice fruit with blueberry residue obtained under this process has the highest comprehensive score of 62.30±0.51. The results of antioxidant test in vitro showed that compared with puffed indica rice fruit, the scavenging rates of DPPH and ABTS by blueberry residue indica rice fruit increased by 60.19% and 73.67% respectively. Conclusion: the optimal processing parameters of indica rice fruit with blueberry residue were obtained, and the product also showed good antioxidant properties.

    • Study on mixing design and freezing resistance optimization of glutinous rice balls

      2022(10):201-209. DOI: 10.13652/j.spjx.1003.5788.2022.90202

      Abstract (412) HTML (0) PDF 2.91 M (382) Comment (0) Favorites

      Abstract:Objective:To improve the poor quality of glutinous rice balls during the freezing process. Methods:The appropriate addition amount of sweet potato starch and wheat starch was obtained through single factor experiment, and then the D-optimal mixture experiment was designed by using sweet potato starch, wheat starch and glutinous rice flour as raw materials to improve the sensory quality and texture characteristics of glutinous rice balls. On the basis of the mixture formula, the effect of deep-sea fish antifreeze protein addition on the frost resistance of glutinous rice balls was explored, and the optimal addition amount was obtained. Results:The optimal mixture formula was 12% sweet potato starch, 11% wheat starch and 77% glutinous rice flour; The suitable addition amount of deep-sea fish antifreeze protein was 5% (calculated by powder weight). Conclusion:The frost resistance of glutinous rice balls made from the mixture formula and antifreeze protein (5%) was obviously optimized, and the overall quality was improved.

    • Effects of Guava leaf extract on the quality and antioxidant capacity of sugar free bread

      2022(10):210-215. DOI: 10.13652/j.spjx.1003.5788.2022.80400

      Abstract (251) HTML (0) PDF 1.68 M (380) Comment (0) Favorites

      Abstract:Objective: In order to develop a sugar-free, antioxidant and low-cost bread. Methods: Guava leaf extract and neohesperidin dihydrochalcone were added as functional ingredients to the bread. The specific volume, texture, water retention and free radical scavenging capacity of bread were tested to analyze its quality and antioxidant capacity. Results: There was no obvious linear relationship between the additive amount of the guava leaf extract and the comprehensive quality of the bread, but the additive amount of guava extract was positively correlated with the total phenolic content, DPPH+ and hydroxyl radical scavenging of bread. When the additive amount of the guava leaf extract was 7.5%, the comprehensive quality of the produced bread was the best. The sensory evaluation reached 78.6 points and the total phenolic content, DPPH+ and hydroxyl radical scavenging rate of the bread were increased to 85%, 70.3% and 141.7%, respectively. The bread had a strong antioxidant capacity. Conclusion: The quality and the sensory score of sugar-free bread treated with Guava leaf extract were increased and the antioxidant capacity has been greatly improved.

    • >ADVANCES
    • Recent studies on the effect of ultrasonic treatment on food allergens

      2022(10):216-223. DOI: 10.13652/j.spjx.1003.5788.2022.90229

      Abstract (742) HTML (0) PDF 1.50 M (570) Comment (0) Favorites

      Abstract:Thisreview introduced the food allergens and their sensitization mechanism, and summarized the research progress of peanut, soybean, milk, shrimp, egg and kiwifruit allergens in ultrasound treatment. Moreover, the research direction of ultrasound treatment in reducing food sensitization was also prospected.

    • Interactions between food polyphenols and proteins and their effects on protein characteristics

      2022(10):224-229. DOI: 10.13652/j.spjx.1003.5788.2022.80504

      Abstract (718) HTML (0) PDF 1.48 M (550) Comment (0) Favorites

      Abstract:This paper summarizes the research progress on the types of interactions between proteins and polyphenols and their effects on protein characteristics, and prospects the future foods with the coexistence of polyphenols and proteins.

    • Research progress on nutritional characteristics and biological activity of bactrian camel milk

      2022(10):230-234. DOI: 10.13652/j.spjx.1003.5788.2022.60071

      Abstract (334) HTML (0) PDF 1.41 M (851) Comment (0) Favorites

      Abstract:In this paper, the composition of protein, amino acids, fatty acids, minerals, vitamins and other nutrients in bactrian camel milk was discussed, and the research progress of the biological activities of camel milk and its enzymolysis products such as hypoglycemic, antibacterial, antiviral and antioxidant activities was summarized.

    • Research status of modern detection technology in automatic liquor picking of Chinese Baijiu

      2022(10):235-240. DOI: 10.13652/j.spjx.1003.5788.2022.90158

      Abstract (342) HTML (0) PDF 1.42 M (621) Comment (0) Favorites

      Abstract:This paper mainly summarized the research status of relevant detection technology in automatic liquor picking since the industrial revolution in China, and prospected its research and application. At the same time, the related research results of influencing liquor quality were summarized.

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