Simultaneous determination of 6 pesticide residues in tea by QuEChERS-GS-MS/MS
CSTR:
Author:
Affiliation:

(Quality Inspection Institute of Quanzhou, Quanzhou, Fujian 362000, China)

Clc Number:

Fund Project:

  • Article
  • |
  • Figures
  • |
  • Metrics
  • |
  • Reference
  • |
  • Related
  • |
  • Cited by
  • |
  • Materials
  • |
  • Comments
    Abstract:

    Objective: This study aimed to establish a method by using QuEChERS-gas chromatography tandem mass spectrometry (GC-MS/MS), to determine six pesticide residues in tea, including: hydroprene, kinoprene, genite, fluronitrofen, cycloprate, and chlornitrofen. Methods: The samples were pretreated by QuEChERS method. They were separated by gas chromatographic, detected by multiple reaction monitoring (MRM) mode and quantified by the external method. Results: All the pesticide residues showed good linearity with correlation coefficients above 0.999 when the concentration falls in the range 0.025~2.000 mg/kg, and the limits of quantitation were in the range of 0.000 6 ~0.007 2 mg/kg. In the recovery experiment of 0.002 5 mg/kg, 0.05 mg/kg, and 0.5 mg/kg at three concentrations, the average recoveries were 84.3%5~116.3%, and the relative standard deviations (RSDs) were 1.07%~6.05%. Conclusion: The method is rapid, simple, and accurate, which is suitable for the detection of these six pesticide residues in tea.

    Reference
    Related
    Cited by
Get Citation

吴汉彬. QuEChERS-气相色谱串联质谱法同时测定茶叶中6种农药残留[J].食品与机械英文版,2023,39(6):55-58,111.

Copy
Share
Article Metrics
  • Abstract:
  • PDF:
  • HTML:
  • Cited by:
History
  • Received:February 28,2022
  • Revised:
  • Adopted:
  • Online: October 20,2023
  • Published:
Article QR Code