Determination of 39 main flavor components in cigarette by ASE—GC/MS
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(1. Research and Development Centre, China Tobacco Jiangxi Industrial Co., LTD., Nanchang, Jiangxi 330096, China; 2. Research and Development Centre, China Tobacco Guangdong Industrial Co., LTD., Guangzhou, Guangdong 510000, China)

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    Abstract:

    The flavor components in 15 domestic cigarettes were extracted with dichlorome-thane by accelerated solvent extraction (ASE), using methyl nonoate as internal standard,a method for semi-quantitative analysis of 39 main flavor components including of acetic acid, 3-Methylbutanoic acid, hexadecoic acid, 2-acetylpyrrole, furfural, furfuryl alcohol, be-nzoic alcohol, phenethyl alcohol, solanone, beta-ionone, phytone, megastigmatrienones (4 isomers), 3-hydroxy-β-damascone, 4-vinyl guaiacol, 5-hydroxy maltol, dihydroactinidiolide et al. by GC/MS/SIM was developped. The results showed that the RSDs ranged from 2.25%~6.49%, the RSD of beta-ionone's determination result was over 5% for the its low content,the other components were below 5%. There was bigger difference between the content of acetic acid, benzoic alcohol, phenethyl alcohol, 2-acetylpyrrole, methyl palmitate,5-hyd-roxy maltol, duvatrendiol in the 15 cigarettes. The method was simple operation, se-nsitive and high in automation, which may be satisfied with the main flavor components detecting requirement of batch cigarettes sample.

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郭磊,李娟娟,索卫国,等.加速溶剂萃取—气质联用法测定卷烟烟丝中39种主要香味成分[J].食品与机械英文版,2017,33(2):60-65,198.

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  • Online: March 10,2023
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