Abstract:The flavor components in 15 domestic cigarettes were extracted with dichlorome-thane by accelerated solvent extraction (ASE), using methyl nonoate as internal standard,a method for semi-quantitative analysis of 39 main flavor components including of acetic acid, 3-Methylbutanoic acid, hexadecoic acid, 2-acetylpyrrole, furfural, furfuryl alcohol, be-nzoic alcohol, phenethyl alcohol, solanone, beta-ionone, phytone, megastigmatrienones (4 isomers), 3-hydroxy-β-damascone, 4-vinyl guaiacol, 5-hydroxy maltol, dihydroactinidiolide et al. by GC/MS/SIM was developped. The results showed that the RSDs ranged from 2.25%~6.49%, the RSD of beta-ionone's determination result was over 5% for the its low content,the other components were below 5%. There was bigger difference between the content of acetic acid, benzoic alcohol, phenethyl alcohol, 2-acetylpyrrole, methyl palmitate,5-hyd-roxy maltol, duvatrendiol in the 15 cigarettes. The method was simple operation, se-nsitive and high in automation, which may be satisfied with the main flavor components detecting requirement of batch cigarettes sample.