真空回转保湿制氮技术在大豆贮藏中的应用
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1.河南工业大学粮食和物资储备学院,河南 郑州 450001;2.武汉东昌仓贮技术有限公司,湖北 武汉 430074;3.商丘市京九粮食储备库,河南 商丘 476299;4.双工方程(武汉)科技发展有限公司,湖北 武汉 430011

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渠琛玲(1982—),女,河南工业大学教授,博士。E-mail:quchengling@163.com

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国家自然科学基金面上项目(编号:32372402); VRM制氮技术在粮食储藏中的应用研究(编号:2024410124000020)


Application of vacuum rotary nitrogen preparation with moisture control in soybean storage
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1.School of Food and Strategic Reserves, Henan University of Technology, Zhengzhou, Henan 450001, China;2.Wuhan Dongchang Storage Technology Co., Ltd., Wuhan, Hubei 430074, China;3.Shangqiu Jingjiu Grain Reserve, Shangqiu, Henan 476299, China;4.Duplex (Wuhan) Technology Development Co., Ltd., Wuhan, Hubei 430011, China

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    摘要:

    目的 为解决传统制氮工艺能耗高、设备体积大、需使用压力容器等问题,研发新型工艺模式下的气调防虫技术,并应用于大豆气调贮藏,有效实现防虫目标。方法 采用一种“常压工况+密闭循环取气”工艺模式下的气调技术(简称真空回转保湿制氮技术)对大豆粮堆(35.7 m×25.6 m×6 m)进行为期3个月的充氮气调,保持98%浓度以上氮气气调28 d,而后保持95%浓度以上气调贮藏至试验结束。对气调过程中充氮降氧效率和仓间低氧维持情况进行监测,评估气调贮藏的杀虫效果;测定充氮前后大豆品质的变化(大豆损伤粒率、水分含量、过氧化值、粗脂肪酸值、碘值、蛋白质溶解比和菌落总数);并分析充氮能耗。结果 降氧阶段充氮仓各层氧气浓度降至杀虫浓度(<2%)共耗时108 h,其中设备运行时长为67 h,低氧维持阶段粮堆各层氧气浓度能在设备不运行的情形下有效维持最长171 h,设备累计运行38 h。低氧(氧气浓度2%以下)维持20 d以上,虫样死亡率100%。充氮前后大豆损伤粒率、水分含量、过氧化值、碘值、蛋白质溶解比和菌落总数均无显著变化,但对照仓和充氮仓中层和下层大豆粗脂肪酸值变化显著(P<0.05),说明氮气气调可延缓大豆酸败。结论 充氮期间,充氮仓的整体吨粮能耗为0.88 kW·h/t,其中降氧阶段为0.55 kW·h/t,低氧维持阶段为0.33 kW·h/t。

    Abstract:

    Objective To solve the problems of high energy consumption, large equipment volume, and the need to use pressure vessels in traditional nitrogen production, this study develops a new pest prevention technology and applies it to the modified atmosphere storage of soybeans to effectively realize pest prevention.Methods Soybeans (pile size: 35.7 m×25.6 m×6 m) are stored for 3 months using a modified atmosphere storage technology under atmospheric pressure with a closed gas cycle, referred to as vacuum rotary nitrogen preparation with moisture control. The concentration of nitrogen is maintained at 98% for 28d, and then at 95% for 2 months. The oxygen reduction efficiency and the maintenance of low oxygen are monitored during the modified atmosphere storage. The insecticidal effect is evaluated, and the changes of soybean quality (including soybean damage rate, moisture content, peroxide value, crude fatty acid value, iodine value, protein solubility ratio, and total colony count) are determined before and after nitrogen filling. Finally, the energy consumption of nitrogen-controlled atmosphere storage (N2-CAS) is analyzed.Results The oxygen concentration of each layer of the soybean pile is reduced to the insecticidal concentration (<2%) within 108 h, during which the equipment operates for 67 h. In the low-oxygen maintenance stage, the oxygen concentration in all layers of the soybean pile is kept stable for up to 171 h without operating the equipment, which only operates for a total of 38 h. When the hypoxia (oxygen concentration of 2% or less) is maintained for 20d, the mortality rate of the insects is 100%. Before and after N2-CAS, there are no significant changes in soybean damage rate, moisture content, peroxide value, iodine value, protein solubility ratio, and total colony count. However, there is a significant difference in the crude fatty acid value of soybeans in the middle and lower layers of the control and N2-CAS (P<0.05) piles. It indicates that N2-CAS is able to delay the rancidity of soybeans.Conclusion The overall energy consumption per ton of the soybean for N2-CAS is 0.88 kW·h/t, including 0.55 kW·h/t in the oxygen reduction stage and 0.33 kW·h/t in the low oxygen maintenance stage.

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宁乐乐,刘勇,渠琛玲,等.真空回转保湿制氮技术在大豆贮藏中的应用[J].食品与机械,2025,41(12):117-122.
NING Lele, LIU Yong, QU Chenling, et al. Application of vacuum rotary nitrogen preparation with moisture control in soybean storage[J]. Food & Machinery,2025,41(12):117-122.

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  • 收稿日期:2025-04-21
  • 最后修改日期:2025-08-23
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  • 在线发布日期: 2026-01-13
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