荸荠皮酚类物质超声波辅助提取工艺优化
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(滁州学院生物与食品工程学院,安徽 滁州 239000)

作者简介:

詹歌,男,滁州学院讲师,博士。

通讯作者:

龙门(1987—),女,滁州学院讲师,博士。E-mail: czxy_lm@163.com

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基金项目:

滁州学院校级规划项目(编号:2016GH05);滁州学院生物与食品工程学院实验室开放课题(编号:SWSP201515KF,SWSP201620KF);安徽省大学生创新创业训练计划项目(编号:201710377069)


Optimization of ultrasonidy assisted extraction of phenolic compounds from the peel of Chinese water chestnut
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(School of Biological and Food Engineering, Chuzhou University, Chuzhou, Anhui 239000, China)

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    摘要:

    采用超声波辅助提取荸荠皮中的酚类物质,考察溶剂种类、料液比、提取温度、超声功率及超声时间对酚类物质提取率的影响。在单因素试验的基础上,确定最佳提取溶剂,并利用响应面法优化工艺条件。结果表明,荸荠皮总酚的最佳提取工艺条件为:甲醇提取,料液比1∶15 (g/mL),提取温度55 ℃,超声功率270 W,超声时间55 min,该条件下总酚含量的最大响应值为4.42 mg/g;荸荠皮总黄酮最佳提取工艺条件为:甲醇提取,料液比1∶20 (g/mL),提取温度60 ℃,超声功率240 W,超声时间55 min,该条件下总黄酮含量的最大响应值为15.20 mg/g。

    Abstract:

    The ultrasonic assisted extraction technique was employed to obtain phenolics from CWCP and different factors on the phenolics yield were considered, including the solvent type, ratio of liquid to solid, extracting temperature, ultrasonic power and ultrasonic time. Based on the single factor tests, an appropriate solvent for more consistent extraction of phenolic compounds would be defined, and response surface experiments would be used to optimize the extraction parameters. The results showed that the optimum conditions for total phenolic extraction were determined: ratio of methanol to solid 1∶15 (g/mL), extracting at 55 ℃ for 55 min with, ultrasonic power 270 W. Under the control of these conditions, the yield of total phenolic content (TPC) was 4.42 mg/g. The optimum conditions for total flavonoid extraction were shown as ratio of methanol to solid 1∶20 (g/mL), extracting temperature 60 ℃, ultrasonic power 240 W and ultrasonic time 55 min and the yield of total flavonoid content (TFC) was 15.20 mg/g under these conditions.

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引用本文

詹歌,李凯凯,孙艳辉,等.荸荠皮酚类物质超声波辅助提取工艺优化[J].食品与机械,2018,34(8):153-160.
ZHANGe, LIKaikai, SUNYanhui, et al. Optimization of ultrasonidy assisted extraction of phenolic compounds from the peel of Chinese water chestnut[J]. Food & Machinery,2018,34(8):153-160.

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  • 收稿日期:2018-02-07
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  • 在线发布日期: 2023-03-17
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