喷雾干燥法制备山苍子油微胶囊的研究
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(1. 中南林业科技大学食品科学与工程学院,湖南 长沙 410004;2. 稻谷及副产物深加工国家工程实验室,湖南 长沙 410004)

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付红军(1975—),男,中南林业科技大学讲师,博士。E-mail:hj0730@163.com

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湖南省重点研发计划项目(编号:2015SK20723,2015SK2072);湖南省教育厅优秀青年项目(编号:16B282);湖南省科技计划项目(编号:2012NK3103)


Preparation of microcapsules made of the oil from Litsea cubeba by spray drying method
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(1. College of Food Science and Engineering, Central South University of Forestry and Technology, Changsha, Hunan 410004, China; 2. National Engineering Laboratory for Rice and Byproducts Processing, Changsha, Hunan 410004, China)

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    摘要:

    采用喷雾干燥法制备山苍子油微胶囊,探讨不同壁材对乳液稳定性和山苍子油微胶囊表面形貌的影响,并优化山苍子油微胶囊的制备工艺。扫描电子显微镜观测结果表明,以羟丙基-β-环糊精/阿拉伯胶(HP-β-CD/AG)为壁材制备的山苍子油微胶囊为颗粒大小均匀、流动性好的圆球形,其他壁材制备的山苍子油微胶囊出现凹陷、皱缩和聚集现象。制备山苍子油微胶囊的优化工艺条件为:WHP-β-CD/AGWLCO 6.0,进料流量3.10 mL/min,进风温度171.0 ℃,该条件下山苍子油包埋率为83.80%,包埋率与3个因素之间的二次多项回归模型合理可靠。

    Abstract:

    Litsea cubeba oil microcapsule were prepared by spray drying method. The effect of several shell materials on emulsion stability and surface morphology of microcapsule was investigated, and process conditions of Litsea cubeba oil microcapsule were optimized. The results of scanning electronic microscope (SEM) showed that Litsea cubeba oil microcapsule prepared with hydroxypropyl-β-cyclodextrin/ arabic gum(HP-β-CD/AG) as wall material is similar to smooth spheres with uniform size and good fluidity, and dents, wrinkles and aggregation for microcapsules prepared with other wall materials were observed. The embedding rate of Litsea cubeba oil in microcapsule was 83.80% under optimum conditions of WHP-β-CD/AG:WLCO 6, feed flow rate inlet 3.10 mL/min at air temperature at 171.0 ℃. The quadratic regression model between embedding rate and three factors was found reasonable and reliable.

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付红军,彭湘莲,钟海雁.喷雾干燥法制备山苍子油微胶囊的研究[J].食品与机械,2016,32(11):187-190.
FUHongjun, PENGXianglian, ZHONGHaiyan. Preparation of microcapsules made of the oil from Litsea cubeba by spray drying method[J]. Food & Machinery,2016,32(11):187-190.

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  • 在线发布日期: 2023-03-09
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